Year 2019, Volume 3 , Issue 2, Pages 66 - 72 2019-12-31

The Effect of Substrate Temperature on The Structure and Morphologies of PbS Thin Films Deposited by Ultrasonic Spray Pyrolysis

Emrah SARICA [1] , Vildan BİLGİN [2]


In this work, we aimed to deposit PbS thin films at relatively low temperature and therefore thin films were deposited onto preheated glass substrates at 473 K and 523 K by ultrasonically spraying of equimolar aqueous solution of lead acetate and thiourea. The thickness of deposited thin films was determined by spectroscopic ellipsometry (SE) prior to investigate physical properties of deposited PbS films. In order to investigate structural and morphological properties of PbS thin films, x-ray diffraction (XRD) patterns and Atomic Force Microscopy (AFM) images were obtained. Crystal structure, mean crystallite size, lattice parameters, micro-strain of deposited thin films were evaluated by means of XRD patterns and it was seen that deposited PbS thin films were successfully obtained in polycrystalline form with cubic crystal structure. Also lattice parameter of a  was calculated as 5.866 Å and 5.870 Å for thin films deposited at 473 K and 523 K, respectively. Additionally, the surface roughness of PbS thin films was determined via AFM images as 5.8 nm and 9.9 nm in non-contact mode. The obtained results confirm that deposition of PbS thin films can be successfully achieved at relatively low temperature. 

Ultrasonic Spray Pyrolysis, PbS Thin Films, Structural Properties, Morphological Properties
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Primary Language en
Subjects Engineering
Journal Section Research Articles
Authors

Orcid: 0000-0002-9339-5114
Author: Emrah SARICA (Primary Author)
Institution: BURSA TEKNİK ÜNİVERSİTESİ
Country: Turkey


Orcid: 0000-0002-0937-6763
Author: Vildan BİLGİN
Institution: ÇANAKKALE ONSEKİZ MART ÜNİVERSİTESİ
Country: Turkey


Dates

Publication Date : December 31, 2019

Bibtex @research article { jise641810, journal = {Journal of Innovative Science and Engineering (JISE)}, issn = {}, eissn = {2602-4217}, address = {ursa Technical University, Mimar Sinan Campus, Mimar Sinan Mah. Mimar Sinan Blv. Eflak Cad. No:177 16310 Yıldırım, Bursa / Turkey}, publisher = {Bursa Technical University}, year = {2019}, volume = {3}, pages = {66 - 72}, doi = {}, title = {The Effect of Substrate Temperature on The Structure and Morphologies of PbS Thin Films Deposited by Ultrasonic Spray Pyrolysis}, key = {cite}, author = {SARICA, Emrah and BİLGİN, Vildan} }
APA SARICA, E , BİLGİN, V . (2019). The Effect of Substrate Temperature on The Structure and Morphologies of PbS Thin Films Deposited by Ultrasonic Spray Pyrolysis. Journal of Innovative Science and Engineering (JISE) , 3 (2) , 66-72 . Retrieved from http://jise.btu.edu.tr/en/issue/50983/641810
MLA SARICA, E , BİLGİN, V . "The Effect of Substrate Temperature on The Structure and Morphologies of PbS Thin Films Deposited by Ultrasonic Spray Pyrolysis". Journal of Innovative Science and Engineering (JISE) 3 (2019 ): 66-72 <http://jise.btu.edu.tr/en/issue/50983/641810>
Chicago SARICA, E , BİLGİN, V . "The Effect of Substrate Temperature on The Structure and Morphologies of PbS Thin Films Deposited by Ultrasonic Spray Pyrolysis". Journal of Innovative Science and Engineering (JISE) 3 (2019 ): 66-72
RIS TY - JOUR T1 - The Effect of Substrate Temperature on The Structure and Morphologies of PbS Thin Films Deposited by Ultrasonic Spray Pyrolysis AU - Emrah SARICA , Vildan BİLGİN Y1 - 2019 PY - 2019 N1 - DO - T2 - Journal of Innovative Science and Engineering (JISE) JF - Journal JO - JOR SP - 66 EP - 72 VL - 3 IS - 2 SN - -2602-4217 M3 - UR - Y2 - 2019 ER -
EndNote %0 Journal of Innovative Science and Engineering (JISE) The Effect of Substrate Temperature on The Structure and Morphologies of PbS Thin Films Deposited by Ultrasonic Spray Pyrolysis %A Emrah SARICA , Vildan BİLGİN %T The Effect of Substrate Temperature on The Structure and Morphologies of PbS Thin Films Deposited by Ultrasonic Spray Pyrolysis %D 2019 %J Journal of Innovative Science and Engineering (JISE) %P -2602-4217 %V 3 %N 2 %R %U
ISNAD SARICA, Emrah , BİLGİN, Vildan . "The Effect of Substrate Temperature on The Structure and Morphologies of PbS Thin Films Deposited by Ultrasonic Spray Pyrolysis". Journal of Innovative Science and Engineering (JISE) 3 / 2 (December 2020): 66-72 .
AMA SARICA E , BİLGİN V . The Effect of Substrate Temperature on The Structure and Morphologies of PbS Thin Films Deposited by Ultrasonic Spray Pyrolysis. JISE. 2019; 3(2): 66-72.
Vancouver SARICA E , BİLGİN V . The Effect of Substrate Temperature on The Structure and Morphologies of PbS Thin Films Deposited by Ultrasonic Spray Pyrolysis. Journal of Innovative Science and Engineering (JISE). 2019; 3(2): 72-66.